核壳型二氧化硅色谱填料的研究进展

doi:10.3724/SP.J.1123.2019.08014

色谱 ›› 2020, Vol. 38 ›› Issue (4): 372-382.DOI: 10.3724/SP.J.1123.2019.08014

核壳型二氧化硅色谱填料的研究进展

夏红军¹^,², 刘家玮¹, 白泉¹^,^*()

1. 教育部天然与功能分子化学重点实验室,西北大学现代分离科学研究所,陕西省现代分离科学重点实验室, 西北大学,陕西西安 710069
2. 河南省稀土功能材料重点实验室,周口师范学院,河南周口 466000

收稿日期:2019-08-19 出版日期:2020-04-08 发布日期:2020-12-10
通讯作者: 白泉
基金资助:
国家自然科学基金项目(21874106);国家自然科学基金项目(21545007);国家自然科学基金项目(21605122);陕西省自然科学基金(2018JZ2001);陕西省自然科学基金(2018JQ2011)

Research progress on core-shell silica stationary phases for high performance liquid chromatography

XIA Hongjun¹^,², LIU Jiawei¹, BAI Quan¹^,^*()

1. Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of Ministry of Education, Institute of Modern Separation Science, Key Lab of Modern Separation Science in Shaanxi Province, Northwest University, Xi’an 710069, China
2. Henan Key Laboratory of Rare Earth Functional Materials, Zhoukou Normal University, Zhoukou 466000, China

Received:2019-08-19 Online:2020-04-08 Published:2020-12-10
Contact: BAI Quan
Supported by:
National Natural Science Foundation of China(21874106);National Natural Science Foundation of China(21545007);National Natural Science Foundation of China(21605122);Natural Science Foundation of Shaanxi Province(2018JZ2001);Natural Science Foundation of Shaanxi Province(2018JQ2011)

摘要/Abstract

摘要：

复杂样品的高效快速分离分析是分离科学家所面临的挑战。近年来,核壳型二氧化硅色谱填料以其高效、快速和低背压的特点被广泛用于小分子、大分子和复杂样品的快速分离分析。该文系统综述了二氧化硅核壳色谱固定相快速分离的机理,制备方法及其在小分子、多肽和生物大分子快速分离分析方面的应用,同时对核壳型色谱固定相的发展进行了展望。

关键词: 核壳型色谱固定相, 高效液相色谱, 快速分离分析, 综述

Abstract:

Fast and efficient separation by using high performance liquid chromatography (HPLC) is challenging for a wide range of samples. In recent years, core-shell silica microspheres have been widely investigated and used for highly efficient and fast separation under reasonably low pressure for small solutes, biopolymers, and complex samples. In this paper, the mechanism for fast separation and preparation methods of core-shell silica microspheres are introduced, along with their application for HPLC-based separation of small molecules, peptides, and biological macromolecules in HPLC. The developing trends of using core-shell microspheres in HPLC are also presented.

Key words: core-shell silica microspheres, high performance liquid chromatography (HPLC), fast separation and analysis, review

中图分类号:

O658

夏红军, 刘家玮, 白泉. 核壳型二氧化硅色谱填料的研究进展[J]. 色谱, 2020, 38(4): 372-382.

XIA Hongjun, LIU Jiawei, BAI Quan. Research progress on core-shell silica stationary phases for high performance liquid chromatography[J]. Chinese Journal of Chromatography, 2020, 38(4): 372-382.

图/表 3

参考文献

[1]	Wren S A C, Tchelitcheff P. J Chromatogr A, 2006, 1119: 140
[2]	Shi X, Li G, Liang Z, et al. Chemistry, 2014, 77: 123
[3]	Guiochon G. J Chromatogr A, 2007, 1168: 101
[4]	Svec F. J Chromatogr A, 2010, 1217(6): 902
[5]	Horvath C, Lipsky S R. J Chromatogr Sci, 1969, 7(2): 109
[6]	Horvath C G, Preiss B A, Lipsky S R. Anal Chem, 1967, 39(12): 1422
[7]	Guiochon G, Gritti F. J Chromatogr A, 2011, 1218: 1915
[8]	Kirkland J J. Anal Chem, 1969, 41(1): 218
[9]	Kirkland J J. Anal Chem, 1992, 64(11): 1239
[10]	DeStefano J J, Langlois T J, Kirkland J J. J Chromatogr Sci, 2008, 46(3): 254
[11]	Gritti F, Leonardis I, Shock D, et al. J Chromatogr A, 2010, 1217: 1589
[12]	Ali I, Gaitonde V D, Grahn A. J Chromatogr Sci, 2009, 48(5): 386
[13]	Brice R W, Zhang X, Colón L A. J Sep Sci, 2009, 32(15/16): 2723
[14]	Ali I, Gaitonde V D, Grahn A. J Chromatogr Sci, 2010, 48: 386
[15]	Gritti F, Guiochon G. J Chromatogr A, 2012, 1228: 2
[16]	Ali I, AL-Othman Z A, AI-Za’ abi M. Biomed Chromatogr, 2011, 26: 1001
[17]	Knox J H. J Chromatogr A, 1999, 831: 3
[18]	Hayes R, Ahmed A, Mdge T, et al. J Chromatogr A, 2014, 1357: 36
[19]	Gritti F, Cavazzini A, Marchetti N, et al. J Chromatogr A, 2007, 1157: 289
[20]	Gritti F, Guiochon G. J Chromatogr A, 2011, 1218: 3476
[21]	Gritti F, Guiochon G. J Chromatogr A, 2010, 1217: 5069
[22]	Gritti F. Chromatogr Today, 2012, 5(2): 4
[23]	Wagner B M, Schuster S A, Boyes B E, et al. J Chromatogr A, 2012, 1264: 22
[24]	González-Ruiz V, Olives A I, Martín M A. TrAC-Trends Anal Chem, 2015, 64: 17
[25]	Deridder S, Catani M, Cavazzini A, et al. J Chromatogr A, 2016, 1456: 137
[26]	Bobály B, Veuthey J L, Guillarme D, et al. J Pharmaceut Biomed, 2018, 158: 225
[27]	Blue L E, Jorgenson J W. J Chromatogr A, 2011, 1218(44): 7989
[28]	Kirkland J J, Langlois T J.U.S. Patent, 7056290, 2007-2-13
[29]	Gritti F, Leonardis I, Abia J, et al. J Chromatogr A, 2010, 1217: 3819
[30]	Wu X, You L, Di B, et al. J Chromatogr A, 2013, 1299: 78
[31]	Chen W, Jiang K, Mack A, et al. J Chromatogr A, 2015, 1414: 147
[32]	Spasova M, Salgueiriñomaceira V, Schlachter A, et al. J Mater Chem, 2005, 15(15): 2095
[33]	Dong H, Brennan J D. Chem Commun, 2011, 47(4): 1207
[34]	Dong H, Brennan J D. J Colloid Inter Sci, 2015, 437: 50
[35]	Unger K K, Kumar D, Grün M, et al. J Chromatogr A, 2000, 892: 47
[36]	Schuster S A, Wagner B M, Boyes B E, et al. J Chromatogr Sci, 2010, 48(7): 566
[37]	Guo W, Goh D C, Zhao X S. J Mater Chem, 2005, 15(15): 4112
[38]	Ma Y, Qi L, Ma J, et al. Colloid Surface A, 2003, 229(1/2/3): 1
[39]	Yang L M, Wang Y J, Sun Y W, et al. J Colloid Interf Sci, 2006, 299(2): 823
[40]	Ahmed A, Clowes R, Willneff E, et al. Ind Eng Chem Res, 2009, 49(2): 602
[41]	Xia H J, Wan G P, Chen G, et al. Mater Lett, 2017, 192: 5
[42]	Xia H J, Wang J, Chen G, et al. Microchim Acta, 2019, 186(2): 125
[43]	Martin T, Galarneau A, Renzo F D, et al. Cheminform, 2002, 33(40): 2590
[44]	Galarneau A, Iapichella J, Bonhomme K, et al. Adv Funct Mater, 2006, 16(13): 1657
[45]	Dong H, Brennan J D. J Mater Chem, 2012, 22(26): 13197
[46]	Min Y, Jiang B, Wu C, et al. J Chromatogr A, 2014, 1356: 148
[47]	Min Y, Yang K, Liang Z, et al. RSC Adv, 2015, 5(33): 26269
[48]	Kirkland J J, Truszkowski F A, Dilks C H, et al. J Chromatogr A, 2000, 890: 3
[49]	Ricker R D, Woodward III C B, Forrer K, et al. J Chromatogr Sci, 2008, 46: 261
[50]	Kirkland J J. Anal Chem, 1992, 64(11): 1239
[51]	Chen W, Wei T C.U.S. Patent, 7846337. 2010-12-7
[52]	Chen W, Jiang K, Mack A, et al. J Chromatogr A, 2015, 1414: 147
[53]	Wan G, Xia H, Wang J, et al. Chinese Chem Lett, 2018, 29(1): 213
[54]	Yang X, Wan G, Ma S, et al. Talanta, 2020, 207: 120310
[55]	Polshettiwar V, Cha D, Zhang X, et al. Angew Chem Int Edit, 2010, 49(50): 9652
[56]	Yu K, Zhang X, Tong H, et al. Mater Lett, 2013, 106: 151
[57]	Shen D, Yang J, Li X, et al. Nano Lett, 2014, 14(2): 923
[58]	Qu Q, Min Y, Zhang L, et al. Anal Chem, 2015, 87(19): 9631
[59]	Zuo C Z, Chen Y, Chen A L. Chinese J Mater Res, 2018, 32(10): 791
[60]	Sun Y S, Qu Q S, Yu S X, et al. Chinese Journal of Chromatography, 2016, 34(12): 1249
[60]	孙元社, 瞿其曙, 于淑新, 等. 色谱, 2016, 34(12): 1249
[61]	Wang H, Xue Y, Lu Y F, et al. Chinese Journal of Chromatography, 2015, 31(3): 215
[61]	汪慧, 薛芸, 鲁阳芳, 等. 色谱, 2015, 31(3): 215
[62]	Ahmed A, Ritchie H, Myers P, et al. Adv Mater, 2012, 24(45): 6042
[63]	Ahmed A, Abdelmagid W, Ritchie H, et al. J Chromatogr A, 2012, 1270: 194
[64]	Unger K K, Skudas R, Schulte M M. J Chromatogr A, 2008, 1184: 393
[65]	Gritti F, Cavazzini A, Marchetti N, et al. J Chromatogr A, 2007, 1157: 289
[66]	Majors R E, Wang X L, Carr P W, et al.LC GC N Am, 2010, 28(11): 932
[67]	Ahmad I A H, Soliven A, Allen C, et al. J Chromatogr A, 2015, 1386: 31
[68]	Cunliffe J M, Noren C F, Hayes R N, et al. J Pharmaceut Biomed, 2009, 50(1): 46
[69]	Kirkland J J, Schuster S A, Johnson W L, et al. J Pharm Anal, 2013, 3(5): 303
[70]	He J W, Wen J X, Lai Y H, et al. Chinese Journal of Chromatography, 2018, 36(8): 758
[70]	何嘉雯, 温家欣, 赖宇红, 等. 色谱, 2018, 36(8): 758
[71]	Zhang X Y, Zhang X Y, Cai X X, et al. Chinese Journal of Chromatography, 2017, 35(5): 482
[71]	张晓艺, 张秀尧, 蔡欣欣, 等. 色谱, 2017, 35(5): 482
[72]	Xu J H, Xue Y, Wang Y, et al. Chemistry & Bioengineering, 2017, 34(6): 65
[72]	徐静涵, 薛芸, 王彦, 等. 化学与生物工程, 2017, 34(6): 65
[73]	Armentano A, Summa S, Magro S L, et al. J Chromatogr A, 2018, 1531: 46
[74]	Mao J, Lei S, Yang X, et al. Food Control, 2013, 32(2): 505
[75]	Wu J, Qian Y, Mao P, et al. J Chromatogr B, 2013, 927: 173
[76]	Manns D C, Mansfield A K. J Chromatogr A, 2012, 1251: 111
[77]	Fibigr J, Majorová M, Vlcková H K, et al. J Pharmaceut Biomed, 2018, 151: 291
[78]	Pedrouzo M, Borrull F, Pocurull E, et al.J Sep Sci, 2011, 34(10): 1091
[79]	Gallart-Ayala H, Moyano E, Galceran M T. J Chromatogr A, 2010, 1217: 3511
[80]	Ciofi L, Fibbi D, Chiuminatto U, et al. J Chromatogr A, 2013, 1283: 53
[81]	Fontanals N, Marcé R M, Borrull F. J Chromatogr A, 2011, 1218: 5975
[82]	Hurtado-Sánchez M C, Romero-González R, Rodríguez-Cáceres M I, et al. J Chromatogr A, 2013, 1305: 193
[83]	Chen X L, Li Z X, Cao Z Y, et al. Chinese Journal of Chromatography, 2013, 31(10): 954
[83]	陈小龙, 李正翔, 曹赵云, 等. 色谱, 2013, 31(10): 954
[84]	Cavazzini A, Pasti L, Massi A, et al. Anal Chim Acta, 2011, 706(2): 205
[85]	Lai X, Tang W, Ng S C. J Chromatogr A, 2011, 1218: 5597
[86]	Ward T J, Ward K D. Anal Chem, 2012, 84(2): 626
[87]	Lomsadze K, Jibuti G, Farkas T, et al. J Chromatogr A, 2012, 1234: 50
[88]	Wu X, You L, Di B, et al. J Chromatogr A, 2013, 1299: 78
[89]	Kirkland J J, Truszkowski F A, Dilks C H, et al. J Chromatogr A, 2000, 890: 3
[90]	Schuster S A, Wagner B M, Boyes B E, et al. J Chromatogr Sci, 2010, 48(7): 566
[91]	Fekete S, Guillarme D. J Chromatogr A, 2013, 1320: 86
[92]	Wagner B M, Schuster S A, Boyes B E, et al. J Chromatogr A, 2012, 1264: 22
[93]	Kirkland J J, Schuster S A, Johnson W L, et al. J Pharm Anal, 2013, 3(5): 303
[94]	Sommella E, Pepe G, Ventre G, et al. J Chromatogr A, 2015, 1375: 54
[95]	Roth M J, Plymire D A, Chang A N, et al. Anal Chem, 2011, 83: 9586
[96]	Wang Q, Lacher N A, Muralidhara B K, et al.J Sep Sci. 2010, 33: 2671
[97]	Staub A, Zurlino D, Rudaz S, et al. J Chromatogr A, 2011, 1218: 8903
[98]	Qu Q, Si Y, Xuan H, et al. J Chromatogr A, 2018, 1540: 31
[99]	Gritti F, Guiochon G. J Chromatogr A, 2011, 1218: 907
[100]	Wagner B M, Schuster S A, Boyes B E, et al. J Chromatogr A, 2012, 1264: 22
[101]	Fekete S, Guillarme D. LC GC Eur, 2012, 25: 540
[102]	Fekete S, Dong M W, Zhang T, et al. J Pharm Biomed Anal, 2013, 83: 273
[103]	Bobaly B, Lauber M, Beck A, et al. J Chromatogr A, 2018, 1549: 63
[104]	Wei B, Zhang B, Boyes B, et al. J Chromatogr A, 2017, 1526: 104
[105]	Fekete S, Rodriguez-Aller M, Cusumano A, et al. J Chromatogr A, 2016, 1431: 94

核壳型二氧化硅色谱填料的研究进展

Research progress on core-shell silica stationary phases for high performance liquid chromatography

RichHTML

PDF

可视化

摘要/Abstract

引用本文

使用本文

扫码分享

图/表 3

参考文献

相关文章 15

编辑推荐

Metrics

[1]	史洪飞, 徐伯芃, 徐成鑫, 周修齐, 许宏福. 溶剂萃取-高效液相色谱-四极杆飞行时间质谱法快速提取检测干燥恰特草中5种生物碱成分[J]. 色谱, 2023, 41(9): 771-780.
[2]	周然锋, 张惠贤, 尹小丽, 彭西甜. 新型纳米材料在农产品安全分析中的应用进展[J]. 色谱, 2023, 41(9): 731-741.
[3]	赵芮, 黄晴雯, 余智颖, 韩铮, 范楷, 赵志辉, 聂冬霞. QuEChERS-超高效液相色谱-串联质谱法同时测定水果中36种真菌毒素[J]. 色谱, 2023, 41(9): 760-770.
[4]	刘宇, 邢家溧, 沈坚, 毕晓丽, 毛玲燕, 徐晓蓉, 张书芬, 娄永江, 吴希, 穆应花. 高效液相色谱-蒸发光散射检测法同时测定固态食品中6种稀有糖[J]. 色谱, 2023, 41(9): 781-788.
[5]	岳超, 赵超群, 毛思浩, 王展华, 施贝, 徐欣丰, 梁晶晶. 通过式固相萃取净化-超高效液相色谱-串联质谱法测定液体乳中10种氨基甲酸酯类农药残留[J]. 色谱, 2023, 41(9): 807-813.
[6]	马超, 倪洪星, 戚羽霖. 超高效液相色谱-傅里叶变换离子回旋共振质谱法解析溶解性有机质的化学多样性[J]. 色谱, 2023, 41(8): 662-672.
[7]	曹沁玲, 赵小丹, 沈国滨, 汪竹琴, 章弘扬, 张敏, 胡坪. 基于超高效液相色谱-电雾式检测的槐糖脂指纹图谱[J]. 色谱, 2023, 41(8): 722-729.
[8]	钱正明, 吴梦奇, 谭国英, 金李玲, 李宁, 谢菊英. 高效液相色谱紫外等吸收波长法快速测定秦皮中秦皮甲素和秦皮乙素[J]. 色谱, 2023, 41(8): 690-697.
[9]	吴萍萍, 林仁义, 黄丽英. 三相中空纤维液相微萃取-高效液相色谱法测定铁皮石斛和金线莲中3种植物生长调节剂[J]. 色谱, 2023, 41(8): 683-689.
[10]	孟二琼, 念琪循, 李峰, 张秋萍, 许茜, 王春民. 磺酸化磁性氮化碳固相萃取-超高液相色谱-串联质谱筛检淡水鱼中孔雀石绿和隐色孔雀石绿[J]. 色谱, 2023, 41(8): 673-682.
[11]	陈东洋, 张昊, 张磊, 王一红, 王小丹, 冯家力, 梁静, 钟旋. 固相萃取-超高效液相色谱-串联质谱法测定发酵食品中的曲酸[J]. 色谱, 2023, 41(7): 632-639.
[12]	王秋旭, 冯启言, 朱雪强. 加速溶剂萃取-固相萃取净化结合超高效液相色谱-串联质谱法测定沉积物中双酚类化合物[J]. 色谱, 2023, 41(7): 582-590.
[13]	杨哲, 吕建霞, 吴一荻, 蒋力维, 李冬梅. 超高效液相色谱法同时测定电子烟油中的5种吲哚/吲唑酰胺类合成大麻素[J]. 色谱, 2023, 41(7): 602-609.
[14]	夏宝林, 汪仕韬, 殷晶晶, 张维益, 杨娜, 刘强, 吴海晶. 自动上样固相萃取-超高效液相色谱-串联质谱法同时测定水中9类43种抗菌药物残留[J]. 色谱, 2023, 41(7): 591-601.
[15]	童学智, 陈东洋, 冯家力, 范翔, 张昊, 杨胜园. QuEChERS-超高效液相色谱-串联质谱法快速测定水产品中5种卤代苯醌[J]. 色谱, 2023, 41(6): 490-496.