三嗪基多孔有机材料的合成及在固相微萃取应用中的研究进展

doi:10.3724/SP.J.1123.2020.07036

色谱 ›› 2021, Vol. 39 ›› Issue (2): 125-129.DOI: 10.3724/SP.J.1123.2020.07036

三嗪基多孔有机材料的合成及在固相微萃取应用中的研究进展

王灼, 王文瑾, 张帅华^*(), 王春, 王志^*()

河北农业大学理学院化学系, 河北保定 071001

收稿日期:2020-07-16 出版日期:2021-02-08 发布日期:2021-01-14
通讯作者: 张帅华,王志
作者简介:张帅华:工学博士,副教授,河北农业大学“太行学者”三层次人才,河北省化学会化学教育专业委员会委员,《色谱》杂志青年编委。现任河北农业大学理学院化学系副主任、理学院创新创业教研室主任。2018年至2020年,获国家留学基金委博士后项目资助在日本国立物质材料研究机构(NIMS)材料纳米构造国际中心(WPI-MANA)从事博士后研究工作。主要研究方向为纳米材料的设计合成,固相微萃取、液相微萃取等样品前处理技术,以及在气相色谱、液相色谱、气相色谱-质谱等领域开展了系统的研究工作,在国际著名期刊Adv Sci, Angew Chem, Small, Chem Eng J, Energy Chem和J Chromatogr A等发表SCI论文60余篇,论文SCI总引用次数超过1000次。荣获河北省优秀博士学位论文、河北农业大学自然科学一等奖、河北省科技进步三等奖等。* Tel:(0312)7528291,E-mail: zhangshuaihua@hebau.edu.cn(张帅华);Tel:(0312)7521513,E-mail: wangzhi@hebau.edu.cn(王志).
基金资助:
国家自然科学基金项目(31571925);国家自然科学基金项目(31671930);河北省自然科学基金项目(B2020204001);河北省自然科学基金项目(C2020204136)

Advances in construction of triazine-based porous organic polymers and their applications in solid phase microextraction

WANG Zhuo, WANG Wenjin, ZHANG Shuaihua^*(), WANG Chun, WANG Zhi^*()

Department of Chemistry, College of Science, Hebei Agricultural University, Baoding 071001, China

Received:2020-07-16 Online:2021-02-08 Published:2021-01-14
Contact: ZHANG Shuaihua,WANG Zhi
Supported by:
National Natural Science Foundation of China(31571925);National Natural Science Foundation of China(31671930);Natural Science Foundation of Hebei Province(B2020204001);Natural Science Foundation of Hebei Province(C2020204136)

摘要/Abstract

摘要：

三嗪基多孔有机材料(TPOPs)具有较大的比表面积、可调的孔道结构、较高的热和化学稳定性、丰富的π键体系等诸多优点,目前被广泛应用于气体储存、催化、能源转化和吸附等诸多领域。基于TPOPs的固相微萃取(SPME)技术近年来引起了人们的极大兴趣,成为样品前处理技术领域的研究热点之一。该文简要地综述了近年来TPOPs的合成方法及其在固相微萃取领域的应用与发展,并对该领域研究进行了展望。

关键词: 固相微萃取, 合成, 三嗪基多孔有机材料

Abstract:

The large surface area, adjustable pore structure, good thermal and chemical stabilities, and abundant π-electron systems make triazine-based porous organic polymers (TPOPs) as promising porous materials for gas storage, catalysis, energy conversion and adsorption. Recently, TPOPs have aroused ever-increasing interest and are considered as one of the research highlights in solid phase microextraction (SPME) and other sample pretreatment techniques. This minireview summarizes the recent advancements in the synthesis of TPOPs and their applications in SPME. The application prospects of the TPOPs in SPME and other sample pretreatment techniques are also presented.

Key words: solid phase microextraction (SPME), construction, triazine-based porous organic polymers (TPOPs)

中图分类号:

O658

王灼, 王文瑾, 张帅华, 王春, 王志. 三嗪基多孔有机材料的合成及在固相微萃取应用中的研究进展[J]. 色谱, 2021, 39(2): 125-129.

WANG Zhuo, WANG Wenjin, ZHANG Shuaihua, WANG Chun, WANG Zhi. Advances in construction of triazine-based porous organic polymers and their applications in solid phase microextraction[J]. Chinese Journal of Chromatography, 2021, 39(2): 125-129.

图/表 1

参考文献

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Coating	Samples	Analytes	Analytical method	LOD	Linear range	Ref.
TPT-COF	juice	PAEs	GC-FID	5-95 ng/L	0.01-100 μg/L	[27]
PAF	cosmetics	antioxidants	GC-FID	0.12-0.22 μg/L	0.02-500 mg/L	[28]
		preservatives		0.19-0.30 μg/L
PAF-6	water	PAHs	GC-MS	0.8-4.2 ng/L	1.6-4000 ng/L	[29]
COF-F-1	water	PFASs	nanoESI-MS	0.02-0.8 ng/L	1-5000 ng/L	[30]
PAF-56P	fruits and vegetables	triazole fungicides	GC-MS	0.15-1.70 ng/g	2.50-250 ng/g	[31]
TOPs@SiO₂	water	PAHs	HPLC	0.003-0.010 μg/L	0.010-20 μg/L	[32]
SNW-1	tea leaf, tobacco	VFAs	GC-MS	0.014-0.026 μg/L	0.05-10 μg/L	[33]
	honey	phenols	GC-MS	0.06-0.2 ng/g	0.1-100 ng/g	[34]
CC-TPA	apple, peach and pear	organochlorine pesticides	GC-ECD	0.032-0.090 ng/g	0.11-20 ng/g	[35]
CC-QP	honey	PAHs	GC-MS	0.03-0.19 ng/g	0.10-100 ng/g	[36]
PAF-6-NPC	water	n-alkanes	GC-FID	0.8-6 ng/L	5-2000 ng/L	[38]
	soil			0.01-0.05 ng/g	0.05-20 ng/g

Coating	Samples	Analytes	Analytical method	LOD	Linear range	Ref.
TPT-COF	juice	PAEs	GC-FID	5-95 ng/L	0.01-100 μg/L	[27]
PAF	cosmetics	antioxidants	GC-FID	0.12-0.22 μg/L	0.02-500 mg/L	[28]
		preservatives		0.19-0.30 μg/L
PAF-6	water	PAHs	GC-MS	0.8-4.2 ng/L	1.6-4000 ng/L	[29]
COF-F-1	water	PFASs	nanoESI-MS	0.02-0.8 ng/L	1-5000 ng/L	[30]
PAF-56P	fruits and vegetables	triazole fungicides	GC-MS	0.15-1.70 ng/g	2.50-250 ng/g	[31]
TOPs@SiO₂	water	PAHs	HPLC	0.003-0.010 μg/L	0.010-20 μg/L	[32]
SNW-1	tea leaf, tobacco	VFAs	GC-MS	0.014-0.026 μg/L	0.05-10 μg/L	[33]
	honey	phenols	GC-MS	0.06-0.2 ng/g	0.1-100 ng/g	[34]
CC-TPA	apple, peach and pear	organochlorine pesticides	GC-ECD	0.032-0.090 ng/g	0.11-20 ng/g	[35]
CC-QP	honey	PAHs	GC-MS	0.03-0.19 ng/g	0.10-100 ng/g	[36]
PAF-6-NPC	water	n-alkanes	GC-FID	0.8-6 ng/L	5-2000 ng/L	[38]
	soil			0.01-0.05 ng/g	0.05-20 ng/g

三嗪基多孔有机材料的合成及在固相微萃取应用中的研究进展

Advances in construction of triazine-based porous organic polymers and their applications in solid phase microextraction

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