Chinese Journal of Chromatography

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Analysis of Flavor Compositions of Chinese Distillate Spirits by Fast Gas Chromatography

ZHANG Chao1, HU Keping2, HASHI Yuki1, CAO Lei1, WU Jie3   

  1. 1.Analytical Applications Center, Shimadzu International Trading (Shanghai) Co. Ltd., Beijing 100020, China;
    2.Beijing University of Chemical Technology, Beijing 100029, China;
    3.PetroChina Exploration and Development Research Institute, Beijing 100080, China
  • Received:2007-01-24 Revised:2007-04-25 Online:2007-07-30 Published:1985-06-25

Abstract:

Many kinds of flavor compositions exist in Chinese traditional distillate spirits (liquor), including alcohols, aldehydes, organic acids and esters, the ratios of which decide the flavor and quality of the liquor. In general, these components can be analyzed qualitatively and quantitatively by gas chromatography. However, the traditional analytical method takes longer analysis time. To shorten the analysis time, a fast gas chromatographic method was developed for analyzing the flavor compositions in Chinese liquors. Good results were obtained using a 20 m×0.1 mm×0.1 μm fused-silica capillary column with analysis time within 12 minutes. Moreover, the reproducibility of this method was also very good, and the relative standard deviations (RSDs) of most components were less than 5% except the acids because of their higher boiling points.

Key words: Chinese distillate spirits , flavor compositions, fast gas chromatography