Research progress in hydrothermal carbon materials for separation and analysis

doi:10.3724/SP.J.1123.2019.08026

Abstract

Abstract:

Hydrothermal carbon materials are new functional materials prepared by the hydrothermal reaction of sugars or carbonaceous organic compounds. They have many advantages such as abundant resources of raw materials, environmental-friendliness, hydrophilicity, and easy of modify and so on. These carbon materials have been widely used as catalyst carriers, energy electrode materials, environmental adsorbents, etc. Among these, the application of hydrothermal carbon materials as absorbents reveals their ability to show strong interactions with specific molecules. In recent years, the application of these materials has been gradually extended to the field of chromatography, as stationary phases for solid-phase separation as well as for the enrichment of complex biological samples. In this paper, the recent applications of hydrothermal carbon materials for the analysis of ionic compounds, polar compounds, phosphorylated peptides, and glycopeptides are presented. Finally, the future scope of these materials in separation and enrichment is also discussed.

Key words: hydrothermal carbon, separation, chromatographic stationary phase, enrichment, phosphorylated peptides, glycopeptides, review

CLC Number:

O658

ZHAO Xingyun, ZHANG Hongyan, NIU Huan, WU Ren’an. Research progress in hydrothermal carbon materials for separation and analysis[J]. Chinese Journal of Chromatography, 2020, 38(4): 383-391.

Figures/Tables 6

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Raw material	Synthesis condition	Structure characteristics	Application	Reference
Glucose	160-180 ℃, 4-20 h	200-1500 nm; C=O, OH	encapsulate nanoparticles	[3]
Fructose	120-140 ℃, 0.5-2 h	200-400 nm; containing C=C, C=O, OH	energy storage	[4]
Starch	200 ℃, 12 or 48 h; add Fe₂O₃	2-5 μm; carbon hollow spheres and	carbon fuel cell	[9]
	and Fe(NH₄)₂(SO₄)₂	nanotubes
Cellulose	200-250 ℃, 2 or 4 h	2-10 μm; oxygen-containing groups	catalyst	[7]
Cyclodextrin	180 ℃, 24 h; add F127	0.1-1 μm; hollow mesopore	lithium ion battery	[41]
Sucrose	190 ℃, 5 h; KOH activation	100-150 nm; high BET surface area	supercapacitor	[35]
Glucose	180-200 ℃; add sodium polyacrylate	600-900 nm; monodispersed	catalyst support	[5]
Glucose	150 ℃, 10 h; add NH₃	2-3 μm; amino groups	water purification	[20]
Glucose	190 ℃, 16 h; add sodium polyacrylate	250-500 nm; carboxyl groups	adsorption of heavy metals	[18]
Glucose	180 ℃, 24 h; add 4-aminoacetophenone	0.1-1 μm; oxime groups	adsorption of uranyl ions	[40]
Sucrose	180-250 ℃; add sodium polyacrylate	1-5 μm; monodispersed	ion separation	[42]
Cyclodextrin	170 ℃, 24 h	5 μm; hydrophilic carbon shell	polar compounds separation	[43]
Glucose	180 ℃, 6 h; add VPA, Ti(SO₄)₂	1-8 μm; phosphate group, Ti-IMAC	phosphopeptides enrichment	[44]
Glucose	180 ℃, 6 h; add MSA, MPC	200-1000 nm; MSA, MPC group	glycopeptides enrichment	[45]

Raw material	Synthesis condition	Structure characteristics	Application	Reference
Glucose	160-180 ℃, 4-20 h	200-1500 nm; C=O, OH	encapsulate nanoparticles	[3]
Fructose	120-140 ℃, 0.5-2 h	200-400 nm; containing C=C, C=O, OH	energy storage	[4]
Starch	200 ℃, 12 or 48 h; add Fe₂O₃	2-5 μm; carbon hollow spheres and	carbon fuel cell	[9]
	and Fe(NH₄)₂(SO₄)₂	nanotubes
Cellulose	200-250 ℃, 2 or 4 h	2-10 μm; oxygen-containing groups	catalyst	[7]
Cyclodextrin	180 ℃, 24 h; add F127	0.1-1 μm; hollow mesopore	lithium ion battery	[41]
Sucrose	190 ℃, 5 h; KOH activation	100-150 nm; high BET surface area	supercapacitor	[35]
Glucose	180-200 ℃; add sodium polyacrylate	600-900 nm; monodispersed	catalyst support	[5]
Glucose	150 ℃, 10 h; add NH₃	2-3 μm; amino groups	water purification	[20]
Glucose	190 ℃, 16 h; add sodium polyacrylate	250-500 nm; carboxyl groups	adsorption of heavy metals	[18]
Glucose	180 ℃, 24 h; add 4-aminoacetophenone	0.1-1 μm; oxime groups	adsorption of uranyl ions	[40]
Sucrose	180-250 ℃; add sodium polyacrylate	1-5 μm; monodispersed	ion separation	[42]
Cyclodextrin	170 ℃, 24 h	5 μm; hydrophilic carbon shell	polar compounds separation	[43]
Glucose	180 ℃, 6 h; add VPA, Ti(SO₄)₂	1-8 μm; phosphate group, Ti-IMAC	phosphopeptides enrichment	[44]
Glucose	180 ℃, 6 h; add MSA, MPC	200-1000 nm; MSA, MPC group	glycopeptides enrichment	[45]