Recent advances in graphitic carbon nitride materials for sample pretreatment

doi:10.3724/SP.J.1123.2019.06032

Abstract

Abstract:

As a new type of non-metallic material, graphite carbon nitride (g-C₃N₄) has attracted increasing attention due to its inherent advantages such as simple preparation, excellent thermal and chemical stability, as well as good biocompatibility and non-toxicity. Nowadays, g-C₃N₄ is widely used in electrocatalysis, photocatalysis, biological imaging, and so on. Because of its large specific surface area, π -electron-rich structure, and hydrophobic properties, g-C₃N₄ is considered an ideal candidate material for sample pretreatment. In this work, g-C₃N₄ and its composites as potential sorbents for solid-phase extraction, dispersive solid-phase extraction, magnetic solid-phase extraction, and solid-phase microextraction are reviewed, and the future trends and prospective are discussed.

Key words: graphitic carbon nitride (g-C₃N₄), sample pretreatment, solid-phase extraction (SPE), dispersive solid-phase extraction (d-SPE), magnetic solid-phase extraction (MSPE), solid-phase microextraction (SPME), sorbent, review

HAN Lizhen, YANG Yixin, ZHANG Jing, GUO Jinggong, LU Minghua. Recent advances in graphitic carbon nitride materials for sample pretreatment[J]. Chinese Journal of Chromatography, 2020, 38(1): 28-35.

Figures/Tables 4

Fig. 1 Triazine and tri-s-triazine (heptazine) structures of g-C3N4[13]

Fig. 2 Schematic demonstration of column-assisted dispersive solid-phase extraction (d-SPE) for the analysis of sulfonamides by using MCN as sorbent[47]

Fig. 3 Schematic demonstration for the synthesis and fabrication of a MCN coated SPME fiber[46] EDA: ethylenediamine; CTC: carbon tetrachloride; MCN: mesoporous carbon nitride.

Fig. 4 Schematic demonstration for the synthesis of nano-g-C3N4/CuO and the usage of it as SPME coating for extraction of target analytes[66] g-C3N4: graphitic carbon nitride; SPME: solid-phase microextraction.

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